Ethylenethiourea → HCID 68537668, compound

Participants

Reaction Steps

A mixture of 4-chloro-2-fluorobenzylbromide (0.223 g, 1.0 mmol) and N,N′-ethylene thiourea (0.102 g, 1.0 mmol) in acetonitrile (4.5 ml) was heated for 10 min to 110° C. by microwave irradiation. After cooling down to room temperature a solid precipitated that was removed by filtration and washed with ether. It was obtained 260 mg (80%) of a white solid; MS (ISP): 245.0; 247.0 ([M+H]+.).

Provenance & Evidence