HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 16063636, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 4-Adamantan-1-yl-5-methyl-1-pyridin-2-yl-1,2-dihydro-pyrazol-3-one | HCID 16063634 | — |
| Reactant | 4-Adamantan-1-yl-1-(4-fluoro-phenyl)-5-methyl-1,2-dihydro-pyrazol-3-one | HCID 68678247 | — |
| Product | HCID 16063636 | HCID 16063636 | — |
Reaction Steps
This compound was obtained in two steps in analogy to example 62 and 61 using 4-fluorophenylhydrazine (example 62) and using iodomethane and 4-adamantan-1-yl-1-(4-fluoro-phenyl)-5-methyl-1,2-dihydro-pyrazol-3-one (example 61) to give 4-adamantan-1-yl-1-(4-fluoro-phenyl)-2,5-dimethyl-1,2-dihydro-pyrazol-3-one as a yellow solid. MS (ESI+): 341.3 [M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652057B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-be05aa205d61487f821d0cbb0976b5dc |
| Source note | uspto-grants-2010_01 |