HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 3-hydroxy-4-iodobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 3-Hydroxy-4-iodobenzoic acid | HCID 736854 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | Ethyl 3-hydroxy-4-iodobenzoate | HCID 11087596 | 97% |
Reaction Steps
Dissolve 3-hydroxy-4-iodobenzoic acid (2.02 g, 7.65 mmol) in ethanol saturated with HCl gas (50 ml). Heat the solution under reflux overnight. Evaporate ethanol to yield 3-Hydroxy-4-iodo-benzoic acid ethyl ester compound (97% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652064B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-12082c9ecff34a3aaa8ddbc3082354d4 |
| Source note | uspto-grants-2010_01 |