HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorobenzilate → HCID 131727549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorobenzilate | HCID 10522 | — |
| Reactant | Tropenol | HCID 53629842 | — |
| Product | HCID 131727549 | HCID 131727549 | — |
Reaction Steps
4.3 is prepared analogously to the method according to II.1. Yield: 6.95 g (83% of theory) starting from 6.5 g (0.02 mol) of 3i and 2.78 g (0.02 mol) of tropenol; TLC: Rf value: 0.30 (eluant as in step I.1); melting point: 197° C.-199° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652138B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-27a924268bce48dcaac7dc481c81c76e |
| Source note | uspto-grants-2010_01 |