Benzaldehyde → 2,4-Dichloro-3-benzylidene-aminophenol hydrochloride

HRID 1995023Notes

Reaction equation

HRID 1995023 reaction equation
[ClH:1].[Cl:2][C:3]1[C:8]([NH2:9])=[C:7]([Cl:10])[CH:6]=[CH:5][C:4]=1[OH:11].[CH:12](=O)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[ClH:2].[Cl:1][CH:5]1[C:6](=[CH:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:7]([Cl:10])=[C:8]([NH2:9])[CH:3]=[C:4]1[OH:11]

Participants

3

Reactant 2

HCID 240BenzaldehydeHCID 198981173-Amino-2,4-dichlorophenol hydrochloride

Product 1

HCID 705304972,4-Dichloro-3-benzylidene-aminophenol hydrochloride

Procedure

Analogously to the procedure and data in Examples 1 and 2, 2,4-dichloro-3-aminophenol hydrochloride was reacted with benzaldehyde. The reaction product of this example of this invention had the following characteristic data: IR-spectrum (Kbr) cm-1 : 1692, 1620, 1598, 1582, 1515, 1480, 1450, 1430, 1310, 1205, 1160, 1075, 1030, 930, 905, 890, 872, 830, 805, 745, 700, 685, 650.

Sources & evidence

ORD record
ord-43b93e838fe84cdca53767ae77817c91
Source dataset
uspto-grants-1983_09
Patent number
US04402699

Reaction notes

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