HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178421680, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Thiocarbohydrazide | HCID 2724189 | — |
| Reactant | (1-Methylcyclopropyl)-glyoxylic acid tert-butylamide | HCID 20385839 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178421680 | HCID 178421680 | — |
Reaction Steps
183 g of (1-methylcyclopropyl)-glyoxylic acid tert-butylamide and 112 g of thiocarbohydrazide are added to a mixture of 1 liter of 1 N HCl and 1 liter of ethanol. The mixture is refluxed for 8 hours; it is subsequently cooled and diluted with 2 liters of H2O and the crystals are filtered off with suction. White crystals having a yellow lustre are obtained and these are dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04402733 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-f365690b66db476589ec8909926f4fa5 |
| Source note | uspto-grants-1983_09 |