HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Tetrachloride → HCID 86019929, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 85529818 | HCID 85529818 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86019929 | HCID 86019929 | 84% |
Reaction Steps
Twenty grams of p-aminomethylbenzoic acid hemisulfate was suspended in 400 ml of methylene chloride, and 75 g of phosphorus pentachloride was slowly added to the suspension. The reaction was carried out at 40° to 45° C. for 2.5 hours. The solution was cooled with ice, and 300 ml of carbon tetrachloride was added, followed by filtration to give 18.3 g (yield 84%) of p-aminomethylbenzoyl chloride hemisulfate as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04402975 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-56f1ec8307e44327a7b9b38b440630c8 |
| Source note | uspto-grants-1983_09 |