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HRID1995289

反应详情

EQUATION

反应方程式

HRID 1995289 的结构方程式

REACTANTS

反应物

2
结构：Cl.ClCCN1CC2CCC(CC2)C1
HCID12612326

3-(2-Chloroethyl)-3-azabicyclo[3.2.2]nonane--hydrogen chloride (1/1)

C10H19Cl2N

结构：CCc1ccc2c3c(c(=O)oc2c1)CNCC3
HCID13136919

8-Ethyl-1,2,3,4-tetrahydro-5H-[1]benzopyrano[3,4-c]pyridin-5-one

C14H15NO2

PRODUCTS

生成物

1
结构：CCc1ccc2c3c(c(=O)oc2c1)CN(CCN1CC2CCC(CC2)C1)CC3.Cl.Cl
HCID13189014

未命名化合物

收率 68%

PROCEDURE

实验过程

Prepared by the method described for Example 1 from 8-ethyl-1,2,3,4-tetrahydro-5H-[1]benzopyrano[3,4-c]pyridin-5-one (5.5 g, 0.024 moles) and 3-(2-chloroethyl)-3-azabicyclo(3.2.2)nonane hydrochloride (5.5 g, 0.025 moles). Recrystallization from ethanol gave the product (7.4 g), mp 295°-300° C.

WORKUP

后处理

  1. customPrepared by the method
  2. customRecrystallization from ethanol