HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(2-Chloroethyl)-3-azabicyclo[3.2.2]nonane--hydrogen chloride (1/1) → HCID 13189014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(2-Chloroethyl)-3-azabicyclo[3.2.2]nonane--hydrogen chloride (1/1) | HCID 12612326 | — |
| Reactant | 8-Ethyl-1,2,3,4-tetrahydro-5H-[1]benzopyrano[3,4-c]pyridin-5-one | HCID 13136919 | — |
| Product | HCID 13189014 | HCID 13189014 | 68% |
Reaction Steps
Prepared by the method described for Example 1 from 8-ethyl-1,2,3,4-tetrahydro-5H-[1]benzopyrano[3,4-c]pyridin-5-one (5.5 g, 0.024 moles) and 3-(2-chloroethyl)-3-azabicyclo(3.2.2)nonane hydrochloride (5.5 g, 0.025 moles). Recrystallization from ethanol gave the product (7.4 g), mp 295°-300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404138 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-9f876a4f8ea84952bc05cdb19253cd63 |
| Source note | uspto-grants-1983_09 |