HRID1995290

反应详情

EQUATION

反应方程式

HRID 1995290 的结构方程式

PROCEDURE

实验过程

Prepared by the method described for Example 1 from 8-phenyl-1,2,3,4-tetrahydro-5H-[1]benzopyrano[3,4-c]pyridin-5-one (5.54 g, 0.02 moles) and 3-(2-chloroethyl)-3-azabicyclo(3.2.2)nonane hydrochloride (4.48 g, 0.02 moles). Recrystallization from methanol gave the product (920 mg), mp 260°-265° C. (dec).

WORKUP

后处理

  1. customPrepared by the method
  2. customRecrystallization from methanol