HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 13189022, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 8-Methyl-1,2,3,4-tetrahydro-chromeno[3,4-c]pyridin-5-one | HCID 10608708 | — |
| Reactant | HCID 86739020 | HCID 86739020 | — |
| Product | HCID 13189022 | HCID 13189022 | — |
Reaction Steps
Prepared by the method described for Example 13 from 1,2,3,4-tetrahydro-8-methyl-5H-[1]benzopyrano[3,4-c]pyridin-5-one (2.0 g, 0.009 moles), triethylamine (3.1 ml, 0.022 moles), and 3-(2-chloroethyl-3-azabicyclo[3.2.2]nonane. Recrystallization from ethanol gave the product (1.7 g), mp 155°-157° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404138 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-642b7ea69d64475faca0d5ed55efc662 |
| Source note | uspto-grants-1983_09 |