HRID1995294
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Prepared by the method described for Example 13 from 1,2,3,4-tetrahydro-8-methyl-5H-[1]benzopyrano[3,4-c]pyridin-5-one (2.0 g, 0.009 moles), triethylamine (3.1 ml, 0.022 moles), and 3-(2-chloroethyl-3-azabicyclo[3.2.2]nonane. Recrystallization from ethanol gave the product (1.7 g), mp 155°-157° C.
WORKUP
后处理
- customPrepared by the method
- customRecrystallization from ethanol