HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 13189034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 8-Methyl-1,2,3,4-tetrahydro-chromeno[3,4-c]pyridin-5-one | HCID 10608708 | — |
| Reactant | 3-(2-Chloroethyl)-3-azabicyclo[3.3.1]nonane | HCID 14450312 | — |
| Product | HCID 13189034 | HCID 13189034 | 70.2% |
Reaction Steps
Prepared by the method described for Example 13 from 1,2,3,4-tetrahydro-8-methyl-5H-[1]benzopyrano[3,4-c]pyridin-5-one (3.0 g, 0.014 moles), triethylamine (4.2 ml, 0.030 moles), and 3-(2-chloroethyl)-3-azabicyclo[3.3.1]nonane (3.3 g, 0.015 moles). The reflux time is 72 hours. Recrystallization from ethanol gave the product (3.6 g), mp 150°-152° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404138 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-98900ef4c1c64531836bbe0d7cae05dc |
| Source note | uspto-grants-1983_09 |