反应详情

Prepared by the method described for Example 13 from 9-chloro-1,2,3,4-tetrahydro-8-methyl-5H-[1]benzopyrano[3,4-c]pyridin-5-one (1.2 g, 0.005 moles), triethylamine (1.4 ml, 0.010 moles), and 3-(2-chloroethyl)-3-azabicyclo[3.3.1]nonane hydrochloride (1.1 g, 0.005 moles). Recrystallization from methanol gave the product (1.2 g), mp 147°-149° C.

1. customPrepared by the method
2. customRecrystallization from methanol