HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloropicolinic acid → HCID 178522668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloropicolinic acid | HCID 20812 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178522668 | HCID 178522668 | 25.9% |
Reaction Steps
0.46 g of 6-chloro-2-pyridinecarboxylic acid, 15 ml of thionyl chloride and 0.29 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is recrystallized from a mixture of dimethylformamide and water, whereby 0.17 g of N-(5-tetrazolyl)-6-chloro-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-f99068c1b0ab44e9a29c5a15a006197f |
| Source note | uspto-grants-1983_09 |