HRID1995358

反应详情

EQUATION

反应方程式

HRID 1995358 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1.67 g of 4-methoxy-2-pyridinecarboxylic acid, 20 ml of thionyl chloride and 1.2 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is recrystallized from ethanol, whereby 0.28 g of N-(5-tetrazolyl)-4-methoxy-2-pyridinecarboxamide is obtained.

WORKUP

后处理

  1. customThe crude product thus obtained
  2. customis recrystallized from ethanol