HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxypyridine-2-carboxylic acid → HCID 178493195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxypyridine-2-carboxylic acid | HCID 2050099 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 178493195 | HCID 178493195 | 11.7% |
Reaction Steps
1.67 g of 4-methoxy-2-pyridinecarboxylic acid, 20 ml of thionyl chloride and 1.2 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is recrystallized from ethanol, whereby 0.28 g of N-(5-tetrazolyl)-4-methoxy-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-9ea83bc2ed224695a6656fa8a4daf32b |
| Source note | uspto-grants-1983_09 |