HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 178503233, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Pyridinecarboxylic acid, 5-(methylthio)- | HCID 12782763 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178503233 | HCID 178503233 | 34% |
Reaction Steps
0.36 g of 5-methylthio-2-pyridinecarboxylic acid, 6 ml of thionyl chloride and 0.18 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is recrystallized from a mixture of dimethylformamide and ethanol, whereby 0.17 g of N-(5-tetrazolyl)-5-methylthio-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-493cba7214c0441ab993610185627b17 |
| Source note | uspto-grants-1983_09 |