HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 178522685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-Nitropicolinic acid | HCID 520488 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178522685 | HCID 178522685 | 50.6% |
Reaction Steps
0.72 g of 5-nitro-2-pyridinecarboxylic acid, 13 ml of thionyl chloride and 0.37 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is recrystallized from a mixture of dimethylformamide, ethanol and water, whereby 0.51 g of N-(5-tetrazolyl)-5-nitro-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-fdaf5d8a8a8b42839d574cbf7bfea7a0 |
| Source note | uspto-grants-1983_09 |