HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Butylpyridine-2-carboxylic acid → HCID 178441156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Butylpyridine-2-carboxylic acid | HCID 13209559 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178441156 | HCID 178441156 | 63% |
Reaction Steps
0.52 g of 4-n-butyl-2-pyridinecarboxylic acid, 0.48 g of N,N'-carbonyldiimidazole and 0.27 g of 5-aminotetrazole are treated in the same manner as described in Example 2. The crude product thus obtained is recrystallized from a mixture of dimethylformamide, water and ethanol, whereby 0.45 g of N-(5-tetrazolyl)-4-n-butyl-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-4798a0998e9a4c519002ef43ad901bc9 |
| Source note | uspto-grants-1983_09 |