HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylpicolinic acid → HCID 178426299, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylpicolinic acid | HCID 268757 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178426299 | HCID 178426299 | 9% |
Reaction Steps
1.49 g of 3-methyl-2-pyridinecarboxylic acid, 1.8 g of N,N'-carbonyldiimidazole and 1.2 g of 5-aminotetrazole are treated in the same manner as described in Example 2. The crude product thus obtained is recrystallized from a mixture of dimethylformamide and ethanol, whereby 0.2 g of N-(5-tetrazolyl)-3-methyl-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-7790d016bdce4032a36421c3c1d282df |
| Source note | uspto-grants-1983_09 |