HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,6-Dimethylpicolinic acid → HCID 178426477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,6-Dimethylpicolinic acid | HCID 693295 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178426477 | HCID 178426477 | 40.2% |
Reaction Steps
0.81 g of 4.6-dimethyl-2-pyridinecarboxylic acid, 0.86 g of N,N'-carbonyldiimidazole and 0.54 g of 5-aminotetrazole are treated in the same manner as described in Example 2. The crude product thus obtained is recrystallized from a mixture of dimethylformamide and ethanol, whereby 0.47 g of N-(5-tetrazolyl)-4,6-dimethyl-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-e0e4748b8dad4afeb47f0b38fa5eac70 |
| Source note | uspto-grants-1983_09 |