HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,6-Dimethylpyridine-2-carboxylic acid → HCID 178425851, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,6-Dimethylpyridine-2-carboxylic acid | HCID 13209570 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178425851 | HCID 178425851 | 55.4% |
Reaction Steps
0.55 g of 5,6-dimethyl-2-pyridinecarboxylic acid, 0.77 g of N,N'-carbonyldiimidazole and 0.48 g of 5-aminotetrazole are treated in the same manner as described in Example 2. The crude product thus obtained is recrystallized from a mixture of dimethylformamide and ethanol, whereby 0.44 g of N-(5-tetrazolyl)-5,6-dimethyl-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-84fe1d4b39c2493ba0217a002f3c820b |
| Source note | uspto-grants-1983_09 |