HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 178522656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | 6-Bromopyridine-2-carboxylic acid | HCID 593919 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178522656 | HCID 178522656 | 56.5% |
Reaction Steps
0.89 g of 6-bromo-2-pyridinecarboxylic acid, 0.71 g of N,N-carbonyldiimidazole and 0.41 g of 5-aminotetrazole are treated in the same manner as described in Example 2. The crude product thus obtained is recrystallized from a mixture of dimethylformamide and water, whereby 0.67 g of N-(5-tetrazolyl)-6-bromo-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-2d999320cedb49fd885411f619045b1b |
| Source note | uspto-grants-1983_09 |