HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methoxypicolinic acid → HCID 178490499, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methoxypicolinic acid | HCID 570891 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178490499 | HCID 178490499 | 46.4% |
Reaction Steps
0.48 g of 6-methoxy-2-pyridinecarboxylic acid, 0.51 g of N,N'-carbonyldiimidazole and 0.29 g of 5-aminotetrazole are treated in the same manner as described in Example 2. The crude product thus obtained is recrystallized from a mixture of dimethylformamide, water and ethanol, whereby 0.32 g of N-(5-tetrazolyl)-6-methoxy-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-026878b2fd4c4a278e3344619a644804 |
| Source note | uspto-grants-1983_09 |