HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-6-methylpyridine-2-carboxylic acid → HCID 178426117, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-6-methylpyridine-2-carboxylic acid | HCID 11401023 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178426117 | HCID 178426117 | 68.7% |
Reaction Steps
0.68 g of 4-chloro-6-methyl-2-pyridinecarboxylic acid, 0.67 g of N,N'-carbonyldiimidazole and 0.37 g of 5-aminotetrazole are treated in the same manner as described in Example 2. The crude product thus obtained is recrystallized from a mixture of dimethylformamide and ethanol, whereby 0.65 g of N-(5-tetrazolyl)-4-chloro-6-methyl-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-a4cc4b8d7f424794ad10242e96356b48 |
| Source note | uspto-grants-1983_09 |