HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Benzoic acid, 2-chloro-6-nitro-, methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 22596843 | HCID 22596843 | — |
| Product | Benzoic acid, 2-chloro-6-nitro-, methyl ester | HCID 603613 | — |
Reaction Steps
18.9 gm (86 mmols) of 2-chloro-6-nitro-benzoic acid chloride were added dropwise over a period of 10 minutes to 100 ml of methanol. The reaction mixture was refluxed for 4 hours and then evaporated in vacuo. The residue was treated with a little ice-cold methanol and filtered off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404230 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-b0b3036c90754a2ca210b4863c2ba8d6 |
| Source note | uspto-grants-1983_09 |