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HRID1995402

反应详情

EQUATION

反应方程式

HRID 1995402 的结构方程式

REACTANTS

反应物

2
结构：[K+].[O]=[Mn](=[O])(=[O])[O-]
HCID516875

Potassium permanganate

KMnO4

结构：Cc1c([N+](=O)[O-])cccc1S(N)(=O)=O
HCID23540023

未命名化合物

PRODUCTS

生成物

1
结构：O=C1NS(=O)(=O)c2cccc([N+](=O)[O-])c21
HCID21794366

4-Nitro-1H-1lambda~6~,2-benzothiazole-1,1,3(2H)-trione

C7H4N2O5S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

8.0 gm (37 mmols) of 2-methyl-3nitro-benzene sulfonamide were oxidized with potassium permanganate in water analogous to Example 8. After extraction with ether, evaporation and recrystallization from water 3.8 gm (45% of theory) of the nitro compound were obtained.

WORKUP

后处理

  1. extractionAfter extraction
  2. customwith ether, evaporation and recrystallization from water 3.8 gm (45% of theory) of the nitro compound
  3. customwere obtained