HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Permanganate → 4-Nitro-1H-1lambda~6~,2-benzothiazole-1,1,3(2H)-trione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Permanganate | HCID 516875 | — |
| Reactant | 2-Methyl-3-nitrobenzenesulfonamide | HCID 23540023 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-Nitro-1H-1lambda~6~,2-benzothiazole-1,1,3(2H)-trione | HCID 21794366 | — |
Reaction Steps
8.0 gm (37 mmols) of 2-methyl-3nitro-benzene sulfonamide were oxidized with potassium permanganate in water analogous to Example 8. After extraction with ether, evaporation and recrystallization from water 3.8 gm (45% of theory) of the nitro compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404230 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-ba7a2fcd4a00453092b2ddbd2a64410b |
| Source note | uspto-grants-1983_09 |