HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1995431Generated: October 28, 2026
2-(Methylamino)ethanol → HCID 20488604, compound
https://huagongshe.com/reaction/1995431
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-(Methylamino)ethanol | HCID 8016 | — |
| Reactant | 6-Chloro-2,3-dihydrobenzoxazol-2-one | HCID 29858 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20488604 | HCID 20488604 | — |
Reaction Steps
6-Chlorobenzoxazolinone (20 g) and N-methylethanolamine (17.7 g) in methanol (40 ml) were stirred and heated at 65° C. for 3 hours. The mixture was cooled to ambient temperature, filtered, and the residue was washed with diethyl ether to give the desired urea which melted at 178° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04404356 |
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| Source dataset | uspto-grants-1983_09 |
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| ORD ID | ord-60525ab3d8d84893a60097471cfd8c07 |
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| Source note | uspto-grants-1983_09 |
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