HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 14289569, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 6-Bromo-2(3H)-benzoxazolone | HCID 29859 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14289569 | HCID 14289569 | — |
Reaction Steps
6-Bromobenzoxazolinone (35.1 g) was stirred with 55 ml of a 38% solution of dimethylamine in methanol at 60° C. for 21/2 hours. The mixture was cooled and filtered, and the precipitate was washed with cold methanol to give the desired urea (17.9 g), m.pt. 178° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404356 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-7ae1f060b38a4220b6f46784da137fa3 |
| Source note | uspto-grants-1983_09 |