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HRID1995503

反应详情

EQUATION

反应方程式

HRID 1995503 的结构方程式

REACTANTS

反应物

5
结构：O
HCID962

Water

H2O

结构：O=C(O)C(=O)O
HCID971

Oxalic acid

C2H2O4

结构：[O]=[Sb][O][Sb]=[O]
HCID27652

Antimony trioxide

O3Sb2

结构：[NH4+].[O]=[V](=[O])[O-]
HCID516859

Ammonium metavanadate

H4NO3V

结构：O=C([O-])C(=O)[O-].[O]=[V+2]
HCID21900408

[Ethanedioato(2-)-κO1,κO2]oxovanadium

C2O5V

PRODUCTS

生成物

1
结构：O=[Sb]([O-])([O-])[O-].O=[Sb]([O-])([O-])[O-].O=[Sb]([O-])([O-])[O-].O=[Sb]([O-])([O-])[O-].O=[Sb]([O-])([O-])[O-].[V+5].[V+5].[V+5]
HCID178527203

未命名化合物

PROCEDURE

实验过程

40.0 grams of Sb2O3 were added to a vanadyl oxalate solution prepared by adding 35 grams of oxalic acid (H2C2O4.2H2O) to a warm (~55° C.) aqueous mixture of 16.04 grams of ammonium metavanadate (NH4VO3) in 35 ml of water. The reaction mixture was dried at 110° C. and the vanadium antimonate precursor so obtained was calcined in an air flow at 550° C. for 2 hours.

WORKUP

后处理

  1. customprepared
  2. temperaturea warm
  3. customThe reaction mixture was dried at 110° C.