HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorobenzoyl isocyanate → 1-(2,6-Dichlorobenzoyl)-3-(6-methyl-5-phenyl-2-pyridyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorobenzoyl isocyanate | HCID 12912739 | — |
| Reactant | 6-Methyl-5-phenylpyridin-2-amine | HCID 13502855 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 1-(2,6-Dichlorobenzoyl)-3-(6-methyl-5-phenyl-2-pyridyl)urea | HCID 13242650 | — |
Reaction Steps
2,6-Dichlorobenzoyl isocyanate (650 mg) was reacted with 6-methyl-5-phenyl-2-pyridylamine (500 mg) in 25 ml of ethyl acetate. A precipitate formed which was filtered and confirmed by NMR as the desired product, 219°-220° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04405552 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-59a857496e0e4bd2814e14ecedbe41cc |
| Source note | uspto-grants-1983_09 |