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HRID1995620

反应详情

EQUATION

反应方程式

HRID 1995620 的结构方程式

REACTANTS

反应物

2
结构：O=C=NC(=O)c1c(Cl)cccc1Cl
HCID12912739

2,6-Dichlorobenzoyl isocyanate

C8H3Cl2NO2

结构：Cc1cc(N)nc(C)c1-c1ccccc1
HCID13502854

4,6-Dimethyl-5-phenylpyridin-2-amine

C13H14N2

PRODUCTS

生成物

1
结构：Cc1cc(NC(=O)NC(=O)c2c(Cl)cccc2Cl)nc(C)c1-c1ccccc1
HCID13242654

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

4,6-Dimethyl-5-phenyl-2-pyridylamine (500 mg) and 2,6-dichlorobenzoyl isocyanate (650 mg) were reacted in 25 ml ethyl acetate. A precipitate formed which was filtered, dried, and identified by NMR analysis as the desired product, m.p. 230°-235° C.

WORKUP

后处理

  1. customA precipitate formed which
  2. filtrationwas filtered
  3. customdried