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HRID1995720

反应详情

EQUATION

反应方程式

HRID 1995720 的结构方程式

REACTANTS

反应物

2
结构：CCc1c(C(=O)c2ccccc2OC)n(C(C)=O)c(=O)n1C(C)=O
HCID20487494

未命名化合物

结构：O=S(=O)(O)O.O=S(=O)(O)O.O=S(=O)(O)O.O=S(=O)([O-])O.O=S(=O)([O-])[O-].[P+3]
HCID178527676

未命名化合物

PRODUCTS

生成物

1
结构：CCc1c(C(=S)c2ccccc2OC)n(C(C)=O)c(=O)n1C(C)=O
HCID20487464

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

In 100 ml Toluene are suspended 10 g of 1,3-diacetyl-1,3-dihydro-4-ethyl-5-(2-methoxybenzoyl)-2H-imidazole-2-one and 20 g phosphorus pentasulfate. The mixture is refluxed 6 hours and the solvent evaporated to yield the title compound.

WORKUP

后处理

  1. temperatureThe mixture is refluxed 6 hours
  2. customthe solvent evaporated