HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-diacetyl-1,3-dihydro-4-ethyl-5-(2-methoxybenzoyl)-2H-imidazole-2-one → 1,3-Diacetyl-1,3-dihydro-4-ethyl-5-[2-methoxy(thiobenzoyl)]-2H-imidazole-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-diacetyl-1,3-dihydro-4-ethyl-5-(2-methoxybenzoyl)-2H-imidazole-2-one | HCID 20487494 | — |
| Reactant | HCID 178527676 | HCID 178527676 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1,3-Diacetyl-1,3-dihydro-4-ethyl-5-[2-methoxy(thiobenzoyl)]-2H-imidazole-2-one | HCID 20487464 | — |
Reaction Steps
In 100 ml Toluene are suspended 10 g of 1,3-diacetyl-1,3-dihydro-4-ethyl-5-(2-methoxybenzoyl)-2H-imidazole-2-one and 20 g phosphorus pentasulfate. The mixture is refluxed 6 hours and the solvent evaporated to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04405628 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-38ca479c0a284d4e9ae1b01776b6b2ed |
| Source note | uspto-grants-1983_09 |