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HRID1995722

反应详情

EQUATION

反应方程式

HRID 1995722 的结构方程式

REACTANTS

反应物

2
结构：S=P12SP3(=S)SP(=S)(S1)SP(=S)(S2)S3
HCID14817

Phosphorus pentasulfide

P4S10

结构：CCc1[nH]c(=S)[nH]c1C(=O)c1ccc(F)c(F)c1
HCID20487469

未命名化合物

PRODUCTS

生成物

1
结构：CCc1[nH]c(=S)[nH]c1C(=S)c1ccc(F)c(F)c1
HCID20487524

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

Ten grams of 1,3-dihydro-4-ethyl-5-(3,4-difluorobenzoyl)-2H-imidazole-2-thione in toluene and phosphorus pentasulfide was heated at reflux temperature for 5 hours. Evaporation of the solvent provides the title compound.

WORKUP

后处理

  1. temperatureat reflux temperature for 5 hours
  2. customEvaporation of the solvent