HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus sulfide (P2S5) → HCID 20487524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus sulfide (P2S5) | HCID 14817 | — |
| Reactant | HCID 20487469 | HCID 20487469 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20487524 | HCID 20487524 | — |
Reaction Steps
Ten grams of 1,3-dihydro-4-ethyl-5-(3,4-difluorobenzoyl)-2H-imidazole-2-thione in toluene and phosphorus pentasulfide was heated at reflux temperature for 5 hours. Evaporation of the solvent provides the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04405628 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-1cfa91e2e95c4af68ca9588d8c4ee143 |
| Source note | uspto-grants-1983_09 |