HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycidol → HCID 20487788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycidol | HCID 11164 | — |
| Reactant | HCID 20487780 | HCID 20487780 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1-Hexanol | HCID 8103 | — |
| Product | HCID 20487788 | HCID 20487788 | — |
Reaction Steps
26.8 g (0.1 mole) of 2,7,7,9,9-pentamethyl-2-isopropyl-1-oxa-4,8-diaza-spiro[4.5]decan-3-one and 7.4 g (0.1 mole) of glycidol in 60 ml of hexanol were stirred for 65 hours at 140° C. in a stirring apparatus, using as catalyst 3 drops of concentrated HCl. The mixture was then evaporated on a rotary evaporator and the residue was recrystallized from xylene/methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04405735 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-b6a1ea2decb346ef92074c3ef97a47dd |
| Source note | uspto-grants-1983_09 |