HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 20487950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Butanoic acid, 4-chloro-4-oxo-, ethyl ester | HCID 84648 | — |
| Reactant | Methyl 2-azabicyclo[2.2.1]heptane-3-carboxylate hydrochloride | HCID 20487957 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20487950 | HCID 20487950 | — |
Reaction Steps
Using the method of Example 1, 4.45 g (0.0232 m) of 3-carbomethoxy-2-azabicyclo[2.2.1]heptane hydrochloride and 3-carbethoxypropanoyl chloride were reacted using triethylamine and acetone to give 4.59 g of syrupy 2-(3-carbethoxypropanoyl)-3-carbomethoxy-2-azabicyclo[2.2.1]heptane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04405787 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-29423cf371da479e802f4287a69f04b3 |
| Source note | uspto-grants-1983_09 |