HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70524131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | P-Toluenesulfonylhydrazide | HCID 15303 | — |
| Reactant | 2-benzylcyclohexane-1,3-dione | HCID 608740 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70524131 | HCID 70524131 | 15.8% |
Reaction Steps
1-benzyl cyclohexane-2,6-dione (17.25 g), p-toluenesulfonylhydrazine (16.52 g) in methanol (290 ml) was treated with concentrated HCl (1 ml) and left at room temperature for 48 hours. Evaporation of the solvent under reduced pressure and crystallization of the residue gave 1-benzylcyclohexane-2,6-dione mono-p-toluenesulfonylhydrazone (5 g) m.p. 172°-3° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04405810 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-a0372b8d9c1e4eb79dadf0350633e1d7 |
| Source note | uspto-grants-1983_09 |