HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 54270203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Ethyl Bromide | HCID 6332 | — |
| Reactant | 4-Methylphenyl isocyanate | HCID 69325 | — |
| Reactant | 2,4-Dichlorophenyl isocyanate | HCID 75789 | — |
| Reactant | HCID 54333945 | HCID 54333945 | — |
| Reactant | HCID 54493048 | HCID 54493048 | — |
| Product | HCID 54270203 | HCID 54270203 | 81% |
Reaction Steps
The procedure described in Example 2 was repeated, except that 1.48 g of ethyl thioallophanate were used in place of the methyl thioallophanate, 1.3 g of ethyl bromide were used in place of the methyl iodide and 1.33 g of p-tolyl isocyanate were used in place of the 2,4-dichlorophenyl isocyanate. 2.5 g (yield 81%) of the desired compound were obtained in the form of colourless prisms having a melting point of 110°-112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04406687 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-7a8ad13a7dc7462084f1b132b42ecbe1 |
| Source note | uspto-grants-1983_09 |