HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Cresol → 2,6-Dimethylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | TIN OXIDE (SnO) | HCID 88989 | — |
| Catalyst | Manganese oxide | HCID 160959 | — |
| Catalyst | Chromium oxide | HCID 165971 | — |
| Catalyst | Ferrous oxide | HCID 449809 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2,6-Dimethylphenol | HCID 11335 | — |
Reaction Steps
o-cresol, methanol and water in a molar ratio of 1:2,5:2,5 were reacted as described in Example 1. The catalyst contained iron oxide, tin oxide, chromium oxide and manganese oxide in a molar ratio of 100:2:1:1. After working up, 2,6-xylenol was obtained with a selectivity of 98,7%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04406824 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-f8e733f9f9134633bec3cceaa208decb |
| Source note | uspto-grants-1983_09 |