HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 22446281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Diethyl chlorobutanephosphonate | HCID 14665078 | — |
| Reactant | HCID 19689203 | HCID 19689203 | — |
| Product | HCID 22446281 | HCID 22446281 | — |
Reaction Steps
4 g (0.018 mol) of 1-ethoxymethylxanthine were stirred at 70° C. for 6 hours with 3 g of potassium carbonate and 4.9 g (0.0214 mol) of diethyl chlorobutanephosphonate. The solution was filtered and concentrated, and the residue which remained was chromatographed (eluent: dichloromethane/methanol 20:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728686 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-8750cc7ad61a432da65104ddaeebb4b3 |
| Source note | uspto-grants-1998_03 |