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HRID1998

反应详情

EQUATION

反应方程式

HRID 1998 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CCCC(Cl)P(=O)(OCC)OCC
HCID14665078

未命名化合物

结构：CCOCn1c(=O)[nH]c2nc[nH]c2c1=O
HCID19689203

未命名化合物

PRODUCTS

生成物

1
结构：CCOCn1c(=O)c2c(ncn2CCCCP(=O)(OCC)OCC)n(C)c1=O
HCID22446281

未命名化合物

PROCEDURE

实验过程

4 g (0.018 mol) of 1-ethoxymethylxanthine were stirred at 70° C. for 6 hours with 3 g of potassium carbonate and 4.9 g (0.0214 mol) of diethyl chlorobutanephosphonate. The solution was filtered and concentrated, and the residue which remained was chromatographed (eluent: dichloromethane/methanol 20:1).

WORKUP

后处理

  1. filtrationThe solution was filtered
  2. concentrationconcentrated
  3. customthe residue which remained was chromatographed (eluent: dichloromethane/methanol 20:1)