HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2-methylbutane → Diethyl [4-(1-(3-methylbutyl)-3-methylxanthin-7-yl)butyl]phosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2-methylbutane | HCID 12015 | — |
| Reactant | 7-(4-Diethylphosphonobutyl)-3-methylxanthine | HCID 15382433 | — |
| Product | Diethyl [4-(1-(3-methylbutyl)-3-methylxanthin-7-yl)butyl]phosphonate | HCID 22446280 | — |
Reaction Steps
The title substance was prepared from diethyl [4-(3-methylxanthin-7-yl)-butyl]phosphonate and 2-methylbutyl chloride analogously to Example 1 and chromatographed on silica gel (eluent: dichloromethane/methanol 10:1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728686 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-54829741e0d340c6aeb01d34861de329 |
| Source note | uspto-grants-1998_03 |