HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131730940, compound → HCID 131730939, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131730940 | HCID 131730940 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 131730939 | HCID 131730939 | 100% |
Reaction Steps
21 mg of 6-[(4-morpholinophenyl)amino]-4-[(3-nitrobenzyl)amino]pyridine-3-carboxyamide (the compound of Example 102) was dissolved in 1 mL of acetic acid, to which 21 mg of 10% palladium carbon was added, and stirred in a hydrogen atmosphere at room temperature for 4 hours. The 10% palladium carbon was filtered off, and the solvent was evaporated to obtain 19.5 mg (100%) of the title compound as a light gray solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575153B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-1e16bace679549d996fef79173f77c64 |
| Source note | uspto-grants-2013_11 |