HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluorobenzylamine → HCID 58440220, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluorobenzylamine | HCID 145211 | — |
| Reactant | Ethyl 4,6-dichloropyridine-3-carboxylate | HCID 600045 | — |
| Product | HCID 58440220 | HCID 58440220 | — |
Reaction Steps
From 4,6-dichloropyridine-3-carboxylic acid ethylester synthesized according to the method described in US2006/0217417 and 3,5-difluorobenzylamine in a manner similar to Example 1, 6-chloro-4-[(3,5-difluorobenzyl)amino]pyridine-3-carboxylic acid ethyl ester was obtained as a light brown crystalline powder (yield 82%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575153B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-f73ced56cdfc49d7b2fd541b6ef7d014 |
| Source note | uspto-grants-2013_11 |