Potassium Carbonate → HCID 68556559, compound

HRID 2036099Notes

Reaction equation

HRID 2036099 reaction equation
[C:1]1([N:7]2[CH2:12][C:11]3([CH2:17][CH2:16][NH:15][CH2:14][CH2:13]3)[O:10][CH2:9][C:8]2=[O:18])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl[C:20]1[N:21]=[N:22][C:23]([C:26]2[S:30][N:29]=[C:28]([CH3:31])[N:27]=2)=[CH:24][CH:25]=1.C(=O)([O-])[O-].[K+].[K+]>>[CH3:31][C:28]1[N:27]=[C:26]([C:23]2[N:22]=[N:21][C:20]([N:15]3[CH2:14][CH2:13][C:11]4([O:10][CH2:9][C:8](=[O:18])[N:7]([C:1]5[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=5)[CH2:12]4)[CH2:17][CH2:16]3)=[CH:25][CH:24]=2)[S:30][N:29]=1

Participants

4

Reactant 3

HCID 11430Potassium CarbonateHCID 109218293-Chloro-6-(3-methyl-1,2,4-thiadiazol-5-yl)pyridazineHCID 667839244-Phenyl-1-oxa-4,9-diazaspiro[5.5]undecan-3-one

Product 1

HCID 68556559HCID 68556559, compound

Procedure

The object product (147 mg, 49%) was obtained in the same manner as in Example 1 and using 4-phenyl-1-oxa-4,9-diazaspiro[5.5]undecan-3-one (230 mg), 3-chloro-6-(3-methyl-1,2,4-thiadiazol-5-yl)pyridazine (150 mg) and potassium carbonate (140 mg).

Sources & evidence

ORD record
ord-edf063e1201c4e77ad0fff6568d65b39
Source dataset
uspto-grants-2013_11
Patent number
US08575167B2

Reaction notes

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