HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 3-(4-Benzoylpiperazine-1-yl)butane-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Chloro-2-butanone | HCID 20026 | — |
| Reactant | 1-Benzoylpiperazine | HCID 762654 | — |
| Product | 3-(4-Benzoylpiperazine-1-yl)butane-2-one | HCID 68746068 | — |
Reaction Steps
0.05 g (73%) target compound as yellow syrup was yielded on the same method as manufacturing example 10 using 0.05 g (0.26 mmol) 1-benzoylpiperazine, 0.11 g (0.79 mmol, 3.0 eq.) potassium carbonate, 0.03 g (0.26 mmol, 1.0 eq.) 3-chloro-2-butanon.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575173B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-dd2bfa413f504195b33edebe74ad5ed6 |
| Source note | uspto-grants-2013_11 |